Leucaena leucocephala (Lam) de Wit is a fast-growing tree species often used as lead (shade) tree that can be cultivated in Malaysia. This species has potential as an alternative resource for the Malaysian furniture and panel board industries in the coming years because of a shortage of the current frequently used raw material (rubberwood). A study on growth performance and potential as particleboard resource material was done. In terms of growth performance, the preliminary study indicated that Leucaena trees grew at a rate of 44% from the first month to the forth month and 43% from 6 to 12 months. As for particleboard manufacturing, Leucaena: Rubberwood admixture bound with urea formaldehyde (8%, 10%, and 12% resin content) to a density of 700 kg/m3, showed promise of usability when all boards pass the Type P2 board requirement of EN312:2010. In general, L. leucocephala wood is a potential raw material for the manufacture of wood composites.
Variable Climate’s Effect on Wood Material’s Equilibrium Moisture Content in Turkey
Raşit Esen and Caner Türüdü
Some negative attributes of wood material have numerous practical consequences. The most important of these attributes is that wood, as a hygroscopic material, is dependent on the relative humidity of its environment. The hygroscopic nature of wood material can lead to serious problems when used in doors, windows, and interior or exterior decoration materials. The aim of this study was to evaluate the effect on wood materials equilibrium moisture due to different climates in selected provinces in Turkey. This study examined pine (Pinus sylvestris L.) and oak (Quercus borealis L.) woods, both of which are commonly used in industry. Over 12 months, the equilibrium moisture value of these wood was determined in the Bursa, Antalya, İzmir, Malatya, Trabzon, Karabük, Van, and Kars provinces of Turkey. Pine and oak samples, prepared per standards TS 2471 (1976) and TS 2472 (1976), were taken from these provinces each month, and the equilibrium moisture values were determined. It was observed that the use of Scotch pine wood samples for both indoor and outdoor use was more appropriate over the 12-month period. Malatya was the province in which the Scotch pine samples were the least affected. It was also determined that Van was the most suitable province for the interior use of oak wood material. It was not found that indoor use gave better results than outdoor use.
Keywords: Scotch pine; Oak; Wooden material; Equilibrium moisture value
Contact information: Karabük University, Fine Arts Faculty, Department of Industrial Product Design Safranbolu/Karabük 78600, Turkey; *Corresponding author: email@example.com
Wood material has been used since the beginning of civilization and is the oldest building material possessing advantageous properties used by people for heat, shelter, and cooking (Özalp et al. 2009). It is important to know the locale where wood material is destined for use, and the climatic conditions of that area. The time of wood drying, or relative humidity can be adjusted to suit the equilibrium moisture for that climate. In many countries, the equilibrium moisture value changes in wood across various uses have been investigated (Üçüncü et al. 2017). The equilibrium moisture of wood materials depends on the temperature and relative humidity of the ambient air (Simpson 1998). At the same time, the wood’s type (hardwood, softwood, etc.) and structure, specific gravity, material dimensions, cutting shapes, and drying moisture values have been found to affect the value of equilibrium moisture (Şenel 1993; Enayati and Hosseinabadi 2007).
Because of its hydroscopic and anisotropic structure, wood can give and receive moisture depending on the relative humidity and temperature of the environment. As a result of moisture exchange, dimensional expansion and contraction ratio of the wood are direction-dependent due to parallel, radial, and fiber constructions (Gündüz 2007). One of the most fundamental challenges of wood as a hydroscopic material is determining how to minimize the dimensional change that occurs as the material is dried until the equilibrium moisture content reaches the level that fits the material’s usage (Kollmann and Cote 1968; FPL 2010). Introducing the wood material to the equilibrium moisture changes according to the temperature and relative humidity of the environment is important.
Unprotected wood material does not have sufficient natural resistance to different environmental factors in the field of use. It can undergo physical and chemical damage (abiotic, herbal, and animal effects) that destroy the wood (Tsoumis 1991; Eaton and Hale 1993). Engineering solutions should be presented to increase the natural resistance of wood material. In this perspective, it is necessary to determine the kind of attack mechanism against wood material for both outdoor and indoor environments (Highley et al. 1994; Leicester et al. 2003; Creemers et al. 2002).
Various scientific research has shown that the physical and mechanical properties of wood material change depending on the equilibrium moisture value (Devi et al. 2003; Cai et al. 2007; Rowell et al. 2009; Gabrielli and Kamke 2010; Sönmez et al. 2010; Kocaefe et al. 2015; Gupta et al. 2016). To minimize the equilibrium moisture value of wood material, various surface coverings, top surface treatments, impregnation, or heat treatment applications have been performed. It has been reported that the top surface treatment of wood material affects the value of equilibrium moisture positively (Üçüncü et al. 2017). In addition, in some studies, environmental or laboratory conditions were controlled and the wood moisture equilibrium in the wood material was determined in terms of wood moisture value in temperature and moisture levels (Macias Esparza et al. 1990). To reach the equilibrium moisture value of the wood material, the climatic conditions, such as the humidity of the environment where a tree is cut, or the temperature of the environment where a tree is located, affect many factors, such as the location of the wood species (hard or softwood) . For this reason, the equilibrium moisture value of wood material was studied in different locations and in different wood material species.
Many scientific studies have shown that the equilibrium moisture value of wood material can be achieved only in a climate cabinet or laboratory conditions. In this study, the objective was to determine the equilibrium moisture content of wood material over one year, using the samples obtained from Scotch pine and oak wood material, the types of wood most used in the furniture and most wood industrial fields.
The most widely used species, both indoors and outdoors, are Scotch pine (Pinus sylvestris L.) and oak (Quercus borealis Lipsky) wood materials. For this study, the wood materials were obtained from timber in the Karabük province (Karabuk/Turkey). The wood materials cut for test samples were carefully selected to ensure they had not acquired defects, such as decay fungus, from the forest.
Preparation of test samples
To prepare the test specimens, the annual rings of the knotless fibrous rings made of first-class wood material were positioned so that their surfaces were perpendicular to the cracks and prepared the sapwood part according to the principles of TS 53 (1981) and TS 2470 (1976).
To determine the equilibrium moisture value, pine and oak wood materials were prepared according to the TS 2471 (1976) and TS 2472 (1976) principles for both indoors and outdoors, including every wood species for one month (measuring 20 × 20 × 30 mm3). In total, 1,920 indoor and 1,920 outdoor samples test samples were prepared.
Determination of equilibrium moisture
The wood samples were conditioned at 12% humidity in the air (20 ± 2 °C and 65% ± 5% for relative humidity) conditioning cabinet until it reached a constant weight. For the moisture value of each sample, the average humidity was chosen randomly according to the principles specified by TS 2471 (1976). For 10 samples chosen randomly, the humidity levels determined included 9.5% ± 0.5, 10.5% ± 0.5, and 12% ± 0.5.
The balance of moisture by drying methods was determined using automatic temperature controlled by a drying cabinet, and judgment by the operator. The balance should be accurate for samples with a dry weight of approximately 10 g for the samples of 0.001 g, and for 100-g samples for 0.1 g (Kantay 1986). The moisture test sample was taken from wood material. The wet weight was determined by weighing in wet form. The full drying weight was found in a special drying cabinet in 103 ± 2 °C.
Determination of density
To determine the density of test specimens, wood materials were prepared according to the principles specified in TS 2472 (1976). A total of 20 specimens were prepared for each tree sample, 20 × 20 × 30 mm3 in size for the two species. These test samples were weighed on scales with 0.001 g accuracy (m12). Thus, 12% moisture weights of the samples were obtained. Then, the samples were measured using a 0.01-precision digital caliper, and their volumes were calculated (V12). The densities of the test samples obtained (δ12) were determined from the following equation:
δ12 = m12/V12 (g/cm3) (1)
These specimens prepared to determine the equilibrium moisture value were placed in Bursa, Antalya, İzmir, Malatya, Trabzon, Karabük, Van, and Kars provinces in open areas, and in closed areas that prevented exposure to sunlight or any outdoor conditions. Problems that could have arisen by making the specified numbered coding on all test samples determined to avoid mixing the samples were solved. Every month, the samples taken from the indoor and outdoor sites were brought to the laboratory in special hermetic packages. The samples were measured using scales with 0.001-g accuracy, at Karabük University Forest Industry Engineering Laboratory. Weight changes were noted to determine the value of equilibrium moisture change. The samples were dried until they reached an oven dry weight of 103 ± 2 °C to determine the moisture value in the wood material as per TS 2472 (1976). This procedure reduces the samples’ moisture value to 0 at equilibrium that the sample is assumed to have attained its dry weight (Skaar 1988).
The regions and their respective cities with different climatic conditions where the experiments occurred and where the samples were observed can be seen on the map of Turkey in Fig. 1.
Fig. 1. The cities in the experiment’s regions of application
The experiment application areas were observed starting in April 2016, in both indoor and outdoor sites in the designated locations in the provinces shown in Fig. 1. Until April 2017, the moisture samples taken from the environment or given to the environment were calculated as a percentage, measured by test samples brought to the laboratory every month. The most important factor affecting the balance of equilibrium moisture value of the wood was the relative humidity of the environment. Monthly average temperature of the provinces and humidity values for the duration of the experiments are given in Fig. 2 (TSMS 2020).
Fig. 2. 12-month average temperature values
The monthly relative humidity rate values of the provinces for the duration of the experiments are given Fig. 3 (TSMS 2020).
Fig. 3. 12-month average moisture values
Data for each test were statistically analyzed by SPSS 20 version. Analysis of variance was used to test the significance between factors and levels. When the analysis of variance pointed a significant difference among the factors and levels, a comparison of the means was conducted employing a Tukey test.
RESULTS AND DISCUSSION
According to the principles specified in the standard TS 2472 (1976), density values were determined in the Scotch pine and oak wood material obtained from the test specimens in the air-dried state. The air density values of the test samples were obtained as 0.49 g cm3 of Scotch pine and 0.56 g cm3 of oak wood material.
Scotch pine and oak wood from the experimental samples obtained from the climatically different regions of Bursa, Antalya, İzmir, Malatya, Trabzon, Karabük, Van, and Kars provinces reached the 12% equilibrium moisture value, and they were kept at the indoor and outdoor sites for 12 months. Moisture change amounts were determined by taking samples from both types of sites every month from each province. Averages of the change in moisture in Scotch pine samples over the 12-month period are given in Table 1.
According to the average values in Table 1, the pine wood material’s highest equilibrium moisture content of 23.0% was obtained in the interior of Trabzon province in December 2016. The lowest moisture value, 0.06%, was obtained in the indoor sample in August 2016, in Bursa. Similar results were achieved when compared with previous studies (Källander and Landel 2007; Mateo and Alejandra 2015).
Test specimens obtained from Scotch pine wood materials were kept in both indoor and outdoor places in eight different provinces for 12 months. The test specimens were transported regularly in laboratory conditions with special packages sealed from air humidity. Monthly equilibrium moisture values of the test samples were calculated (Figs. 4).
Table 1. Scotch Pine Wood Material at 12-Month Averages of Equilibrium Moisture Values (%)
Fig. 4. The balance equilibrium moisture values of Scotch pine material (indoor and outdoor sites)
According to Fig. 4, the highest humidity value was obtained from the interior of Trabzon province; the lowest humidity value was obtained indoor Bursa.
Table 2. 12-Month Equilibrium Moisture Values of Oak Wood Material (%)
When the data in Table 2 were examined, the average equilibrium moisture value of the oak wood test samples was the highest in May 2016, in Antalya, at 13.5%. The least change in equilibrium moisture value was obtained from the experimental groups in outdoor sites in İzmir, in July 2016, at 0.12%.
Test specimens obtained from oak wood materials were kept in both indoor and outdoor places in eight different provinces for 12. These values are given in Fig. 5. The results of the experimental study showed that the value of equilibrium moisture content in indoor and outdoor sites, in eight different provinces (Antalya, Bursa, İzmir, Karabük, Kars, Malatya, Trabzon, and Van), varied between 0.12% and 13.5%. Oak wood material exhibited values of moisture content that were less than those of Scotch pine. However, as stated in the literature, even if the high density of leafy wood materials absorbs a small amount of moisture, the coefficient of expansion is high (Örs and Keskin 2000).
Fig. 5. The balance moisture values of oak wood tree materials (indoor and outdoor sites)
An analysis of variance was performed to determine whether the interaction between pine and oak wood material experimental groups and the time and place of each had an effect on the equilibrium moisture change of the test samples. The results of the analysis of variance are given in Table 3.
Table 3. Results of the Analysis of Variance
a R2 = 0.862 (Adjusted R2= 0.835)
Factor A: province; Factor B: time; Factor C: place; Factor D: wood type
According to the analysis of variance, provincial space, and application time of the experimental groups, the applied wood type experiments were statistically significant between each other and their interactions with each other (95% significance level P < 0.05). To determine which applications were affected by the difference between the equilibrium moisture value of the test specimens, the Duncan test was performed. The Duncan test results of the tree species are given in Table 4.
Table 4. Provincial Duncan Test Results of Wood Species (Excluding Time and Places)
HG: Homogenous group
When the Duncan test values in Table 4 were examined, the highest humidity value was found in the Trabzon province in Scotch pine samples with 6.74%, and the lowest humidity value was found in the Malatya province in Scotch pine samples with 2.58%. The results of the Duncan test related to the relationship between the wood and the site of application are given in Table 5.
Table 5. Results of the Duncan Test Related to the Relationship Between the Wood and the Applied Province (Excluding Time and Site)
In light of the data obtained from the Duncan test, the highest equilibrium humidity value change was obtained from the pine wood material test group with a value of 3.51% (Table 5). The tree type implementation time interactive Duncan test results are given in Table 6.
According to the data from Table 6, the samples obtained from the oak wood samples in August 2016 were the lowest balance humidity value at 0.37%. In January 2017, the highest equilibrium moisture content was achieved at 10.67% in test samples obtained from Scotch pine material. The results obtained were similar to other academic studies (Yapıcı et al. 2013; Yörür et al. 2017).
Table 6. Duncan Test Results of the Tree Type Implementation (Excluding Time and Site)
HG: Homogenous group
- When the first interactive results of wood species were examined, the highest equilibrium moisture content of 6.74% was obtained from Scotch pine sample groups from the Trabzon province. This high value is attributed to the structure of Scotch pine wood, which has relatively high moisture value caused by the amount of space in the cell wall. At the same time, the average monthly moisture content for a long period of the year, during the experiments were conducted, affected its high value. The lowest equilibrium moisture value was found in the Malatya province at 2.58%. When the average annual relative humidity rate value of the Malatya province was examined, Malatya had the lowest moisture. According to these results, the Malatya province is suggested as the most suitable province for the production of reinforcement elements made from Scotch pine wood material. However, it was observed that pine wood material was not suitable for outdoor use without any protection process in the Malatya province.
- Due to the wide vessels of the oak tree and its anatomical structure, it was thought that the greater the amount of relative humidity in outdoor environments, compared with interior ones, the more the dimension stability will change, depending on the moisture value of the wood material. This aspect of wood material negatively affected the wooden materials (furniture, cabinets, door, etc.). It was thought that the use of oak wood could have negative consequences from exposure in an outdoor environment.
- The lowest value of equilibrium moisture change according to the application time of the experiment was obtained in August 2016 at 0.37%. The highest value of equilibrium moisture change was obtained from Scotch pine test samples in January 2017 (10.67%). The lowest equilibrium humidity in January was due to the average temperature and the relative humidity at the lowest level in this month.
- This study showed that reaching the equilibrium moisture value of the wood material varied depending on the temperature and humidity throughout the seasons, geographical region, and type of the tree. In addition, even on a monthly basis, the moisture content of some wood species varied.
The authors wish to thank the Forestry Faculty and Forestry Industrial Engineering Department at Karabuk University. They also would like to acknowledge support from the Turkish State Meteorological Service (TSMS).
Cai, X., Riedl, B., Zhang, S. Y., and Wan, H. (2007). “Effects of nanofillers on water resistance and dimensional stability of solid wood modified by melamine-urea-formaldehyde resin,” Wood and Fiber Science 39(2), 307-318.
Creemers, J., De Meijer, M., Zimmermann, T., and Sell, J. (2002). “Influence of climatic factors on the weathering of coated wood,” Holz als Roh- und Werkstoff 60, 411-420. DOI: 10.1007/s00107-002-0338-5
Devi, R. R., Ali, I., and Maji, T. K. (2003). “Chemical modification of rubber wood with styrene in combination with a crosslinker: Effect on dimensional stability and strength property,” Bioresource Technology 88(3), 185-188. DOI: 10.1016/S0960-8524(03)00003-8
Eaton, R. A., and Hale, M. D. C. (1993). Wood: Decay, Pests, and Protection, Chapman and Hall, London, England.
Enayati, A. A., and Hosseinabadi, H. Z. (2007). “Determination of equilibrium moisture content (EMC) of wood in the neighboring countries of Iran,” Iranian Journal of Natural Resources 60(3), 1037-1048.
Forest Product Laboratory (2010). Wood Handbook – Wood as Engineering Material, General Technical Report FPL-GTR-190, U.S. Department of agriculture, Forest Service Madison, WI.
Gabrielli, C. P., and Kamke, F. A. (2010). “Phenol-formaldehyde impregnation of densified wood for improved dimensional stability,” Wood Science and Technology 44, 95-104. DOI: 10.1007/s00226-009-0253-6
Gündüz, G. (2007). “Mapping climate index on wood preservation: Case of Turkey,” ZKÜ Bartın Forestry Journal 9(11), 26-33.
Gupta, S., John, A., and Kumar, V. S. K. (2016). “Studies on effect of coat thickness on the moisture uptake by a hardwood substrate,” Maderas. Ciencia y Tecnología 18(3), 443-456. DOI: 10.4067/S0718-221X2016005000040
Highley, T. L., Micales, J. A., Illman, B. L., Green, F., Croan, S. C., and Clausen, C. A. (1994). Research on Biodeterioration of Wood, 1987-1992: II. Diagnosis of Decay and In-Place Treatments (Research Paper FPL–RP–530), U.S. Department of Agriculture Forest Products Laboratory, Madison, WI, USA.
Källander, B., and Landel, P. (2007). “Effects of heat treatment of small clearwood samples on equilibrium moisture content and deformation,” in: COST E 53 Conference – Quality Control for Wood and Wood Products, Warsaw, Poland, pp. 63-68.
Kantay, R., (1986). “The equilibrium moisture and measure of wood material,” İstanbul Üniversisty, Forestry Faculty Journal, B 36(2), 58-74.
Kocaefe, D., Huang, X., and Kocaefe, Y. (2015). “Dimensional stabilization of wood,” Current Forestry Reports 1, 151-161. DOI: 10.1007/s40725-015-0017-5
Kollmann, F. P., and Cote, Jr., W. A. (1968). Principles of Wood Science and Technology, Springer-Verlag, Berlin, Germany. DOI: 10.1007/978-3-642-87928-9
Leicester, R. H., Wang, C.-H., Foliente, G. C., Thornton, J. D., Johnson, G. C., Cause, M., and MacKenzie, C. (2003). “An Engineering models for decay of timber in-ground contact,” in: Proc. Conference of International Research Group 34: Section 2, Paper No. IRG/WP/03, 18-23 May, Brisbane, Australia, 21 pages.
Macias Esparza, E. B., García Bernal, H. R., and Galvis, V. J. A. (1990). “Determination of equilibrium humidity in Panela,” Agronomía Colombiana 7(1-2), 70-75.
Mateo, G. G., and Alejandra, B. R. P. (2015). “Equilibrium moisture content and sorption isotherms determination for different conditions of relative humidity and temperature in the bamboo guadua Angustifolia Kunth,” in: Proceedings of Construction for Sustainability – Green Materials & Technologies, 16.Nocmat, Winnipeg, Canada.
Örs, Y., and Keskin, H. (2000). “Wood material knowledge,” Lesson Book, Gazi University Publisher 26(157), 24-39.
Özalp, M., Atligan, A., Esen, Z., and Kaya, S. (2009). “Comparing the resistance and bending in the plywoods which each made with different glues,” Dumlupınar Ünivitesi Fen Bilimleri Dergisi 18, 99-104.
Rowell, R. M., Ibach, R. E., McSweeny, J., and Nilsson, T. (2009). “Understanding decay resistance, dimensional stability and strength changes in heat-treated and acetylated wood,” Wood Material Science & Engineering 4(1-2), 14-22. DOI: 10.1080/17480270903261339
Senel, A. (1993). “The properties of wooden material on drying effects,” Gazi Üniversity Industrial Arts, Educations Faculty Journal 1(1), 59-66.
Skaar, C. (1988). Wood-water Relations, Springer-Verlag Berlin, Heidelberg, Germany. DOI: 10.1007/978-3-642-73683-4
Simpson, W. T. (1998). Equilibrium Moisture Content of Wood in Outdoor Locations in the United States and Worldwide (Research Note FPL-RN-0268), U.S. Department of Agriculture Forest Products Laboratory, Madison, WI, USA.
Sönmez, A., Budakçı, M., and Bayram, M. (2010). “Effect of wood moisture content on adhesion of varnish coatings,” Scientific Research and Essays 4(12), 1432-1437.
TS 53 (1981). “Wood—Sampling and test methods—Determination of physical properties—Wood, sawlogs sawn timber (ICS 79.040),” Turkish Standards Institution, Ankara, Turkey.
TS 2470 (1976). “Wood—Sampling methods and general requirements for physical and mechanical—Wood, sawlogs sawn timber (ICS 79.040),” Turkish Standards Institution, Ankara, Turkey.
TS 2471 (1976). “Wood, determination of moisture content for physical and mechanical tests—Wood, sawlogs sawn timber (ICS 79.040),” Turkish Standards Institution, Ankara, Turkey.
TS 2472 (1976). “Wood—Determination of density for physical and mechanical tests (ICS 79.040),” Turkish Standards Institution, Ankara, Turkey.
Turkish State Meteorological Service (TSMS) (2020). “Cities and holiday resorts,” Turkish State Meteorological Service, (http://www.mgm.gov.tr/eng/forecast-cities.aspx), Accessed 07 April 2018.
Tsoumis, G. T. (1991). Science and Technology of Wood: Structure, Properties, Utilization, Van Nostrand Reinhold, NY, USA.
Üçüncü, K., Aydın, A., Malkoçoğlu, A., and Ay, N. (2017). “Variation of moisture content of some varnished woods in indoor climatic conditions,” Artvin Coruh University Journal of Forestry Faculty 18(2), 192-200. DOI: 10.17474/artvinofd.315555
Yapici, F., Esen, R., Yörür, H., and Likos, E. (2013). “The effects of heat treatment on the modulus of rupture and modulus of elasticity of Scots pine (Pinus sylvestris L.) wood,” NWSA Journal–Technological Applied Sciences 8(1), 1-6.
Yörür, H., Kesik, H. İ., and Şeker, B. (2017). “The impact on the equilibrium moisture content and dimensional change of service life in historic wooden structures,” Journal of Advanced Technology Sciences 6(3), 1308-1314.
Article submitted: February 4, 2020; Peer review completed: May 15, 2020; Revised version received: July 28, 2020; Accepted: July 29, 2020; Published: